Ultracold Neutron Guide-Coating Facility at U.Winnipeg

Abstract

We report the construction and commissioning of a new ultracold neutron (UCN) guide-coating facility at the University of Winnipeg. The facility employs pulsed laser deposition (PLD) to produce diamond-like carbon (DLC) coatings on cylindrical UCN guides up to 1 m in length with a 200 mm outer diameter. DLC is a promising material for UCN transport and storage due to its high real component of the optical potential, low neutron absorption cross section, and low depolarization probabilities. First coating attempts on a full length aluminum UCN guide and matching blank flange were successfully coated with a carbon film with density of 2.3 g/cm$^3$, corresponding to optical potentials of 200 neV, as measured by X-ray reflectometry (XRR). Coating thicknesses were measured to be 90 nm for the UCN guide and 180 nm for the flange with no evidence of delamination. The implementation of a plasma plume collimator and plasma feed back control via a time of flight in vacuum ion probe produced a film with an XRR measured density of 2.8 g/cm$^3$, corresponding to an optical potential of 240 neV. This 80 nm thick film had poor adhesion to the aluminum tube substrate. These results establish a baseline for the coating facility. Ongoing and future work focuses on improving the diamond content of films and adhesion through plasma plume collimation, TOF ion probe feed back, and pre/post treatment methods with the goal of providing high quality DLC UCN guides for the TUCAN experiment at TRIUMF.